#8590. The Role of Total Synthesis in Structure Revision and Elucidation of Decanolides (Nonanolides)

October 2026publication date
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Medicine (all);
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Abstract:
Although modern spectroscopic methods are nowadays routinely used to elucidate the structure of natural products, structural assignments of ten-membered lactones often remain incomplete or are surprisingly often erroneous. In this study, we demonstrate that enantioselective total synthesis is not only an efficient tool for corroborating or revising a proposed structure, but that the synthesis of different stereoisomers as references for gas chromatographic investigations can be a vital part of the structure elucidation process if only minute amounts of material are available.
Keywords:
Chiral-pool; Decanolides; Nonanolides; Structure revision; Ten-membered lactones; Total synthesis

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